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Giulio Arcangeli is a leading figure in analytical chemistry, specializing in the development and automation of sample preparation techniques, particularly solid-phase microextraction (SPME). His research centers on advancing high-throughput, environmentally friendly methods for detecting biomarkers and environmental pollutants. Arcangeli’s major contributions include pioneering fully automated SPME coupled with fast gas chromatography-mass spectrometry (GC-MS), as demonstrated in his highly cited 2011 work on measuring sarcosine and N-ethylglycine in human urine—a method with significant implications for cancer biomarker discovery. His 2022 review of commercially available SPME technologies, with 64 citations, has become a definitive resource for researchers seeking to implement these techniques. Arcangeli also developed an innovative GC-MS method for assessing formaldehyde in workplace atmospheres, addressing critical occupational health and regulatory concerns, as highlighted in his 2017 study. His work has garnered substantial impact, with his top papers accumulating over 145 citations, reflecting their influence on analytical methodology and environmental monitoring. Arcangeli’s achievements underscore his role in advancing automation and miniaturization in analytical chemistry, making complex analyses more accessible and efficient for both laboratory and field applications.